4'-甲氧基-2-硝基联苯合成路线 (共 37 条)
反应条件
1: caesium carbonate / methanol / 2 h / 20 °C / |Inert atmosphere 2: N,N,N',N,-tetramethylethylenediamine; copper(I) bromide; bis(acetylacetonato) palladium / 16 h / 140 °C / |Inert atmosphere View Scheme
参考文献
Cahiez, Gerard; Moyeux, Alban; Gager, Olivier; Poizat, Mael
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 790 - 796
反应条件
1: iodine; magnesium / tetrahydrofuran / 3 h / 30 °C / |Sonication 2: tetrakis(triphenylphosphine) palladium(0) / toluene / 24 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Universiteit Antwerpen; Kuvshinov, Alexandr; Franck, Philippe; Depraetere, Stefaan; Maes, Bert
Patent: EP2662379 A1, 2013 ;
参考文献
Simamura; Migita
Bulletin of the Chemical Society of Japan, 1954 , vol. 27, p. 228,230
参考文献
Makarowa et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 1452,1457; engl. Ausg. S. 1399, 1404
反应条件
5-palladium/activated carbon; hydrogen in tetrahydrofuran; methanol T=40°C; 12 h;
参考文献
Ibarguren, Oier; Zakri, Cecile; Fouquet, Eric; Felpin, Francois-Xavier
Tetrahedron Letters, 2009 , vol. 50, # 36 p. 5071 - 5074
参考文献
The Boots Company
Patent: US5302720 A1, 1994 ;
反应条件
triethyl phosphite 16 h; Heating / reflux;
参考文献
Koninklijke Philips Electronics N.V.
Patent: EP1838671 B1, 2008 ;
Location in patent: Page/Page column 11; 12 ;