5-(4-溴苯基)-2-呋喃甲醛合成路线 (共 22 条)
反应条件
tetrabutylammomium bromide; potassium carbonate; palladium diacetate in water T=20°C; 2 h;
参考文献
Bussolari, Jacqueline C.; Rehborn, Diana C.
Organic Letters, 1999 , vol. 1, # 7 p. 965 - 967
反应条件
1: 4-bromo-aniline With hydrogenchloride; water; sodium nitrite T=0 - 5°C; 2: furfural With ammonium cerium(IV) nitrate in water T=20°C; 7 h;
参考文献
Subrahmanya Bhat; Shivarama Holla
Heterocyclic Communications, 2003 , vol. 9, # 6 p. 625 - 628
反应条件
1: With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 1 h; 2: With hydrogenchloride in water
参考文献
Kim, Seung-Hoi; Rieke, Reuben D.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1984 - 1993
反应条件
copper(l) chloride in water T=20°C; Meerwein arylation; 48 h;
参考文献
Paizs, Csaba; Taehtinen, Petri; Lundell, Katri; Poppe, Laszlo; Irimie, Florin-Dan; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2003 , vol. 14, # 13 p. 1895 - 1904
反应条件
1: 2-(4-bromophenyl)-5-[(prop-2-yn-1-yloxy)methyl]furan With [2-hydroxymethylpyridine][AuCl2] complex in chloroform T=20°C; 1.5 h; 2: N-phenylazodicarboximide in chloroform T=-28°C; Diels-Alder reaction; 8 h; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 10 p. 1743 - 1750
反应条件
CuCl2*2H2O in water; dimethyl sulfoxide T=24 - 26°C; Meerwein arylation;
参考文献
Obushak; Lesyuk; Gorak, Yu. I.; Matiichuk
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 9 p. 1375 - 1381
反应条件
bis-triphenylphosphine-palladium(II) chloride in acetonitrile T=20°C; Stille reaction; 0.5 h;
参考文献
Hosoya, Takamitsu; Aoyama, Hiroshi; Ikemoto, Takaaki; Kihara, Yasutaka; Hiramatsu, Toshiyuki; Endo, Makoto; Suzuki, Masaaki
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 5 p. 663 - 673
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; toluene T=100°C; Suzuki coupling; 4 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 36 p. 7402 - 7417
反应条件
CuCl2·2H2O in water; acetone T=20°C; 12 h;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 61, # 46 p. 10858 - 10863
反应条件
lead; tetrabutylammomium bromide in dichloromethane T=45°C; 4 h; ultrasonication; Title compound not separated from byproducts;
参考文献
Voznyi; Novikov; Khlebnikov; Kostikov
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 5 p. 689 - 695