7-氧杂-7H-苯并[de]蒽合成路线 （共 10 条）
反应条件
caesium carbonate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
T=140°C; Cyclization; 24 h;
参考文献
Terao, Yoshito; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 10 p. 2345 - 2350
反应条件
palladium on activated charcoal
T=340°C;
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
2: palladium/charcoal / 280 - 320 °C
3: concentrated aqueous HBr; glacial acetic acid
4: palladium/charcoal / 340 °C
View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
1: diethyl ether; benzene / 20 °C
3: palladium/charcoal / 280 - 320 °C
4: concentrated aqueous HBr; glacial acetic acid
5: palladium/charcoal / 340 °C
View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
1: diethyl ether; benzene / 20 °C
3: palladium/charcoal / 280 - 320 °C
4: concentrated aqueous HBr; glacial acetic acid
5: palladium/charcoal / 340 °C
View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
1: concentrated aqueous HBr; glacial acetic acid
2: palladium/charcoal / 340 °C
View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
1: palladium/charcoal / 280 - 320 °C
2: concentrated aqueous HBr; glacial acetic acid
3: palladium/charcoal / 340 °C
View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
T=650°C; P=0.005 Torr; 1 h; Flash vacuum pyrolysis;
参考文献
Black, Michael; Cadogan; McNab, Hamish
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 13 p. 2961 - 2967
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
1: ethanol; sodium
2: sodium dichromate; acetic acid
3: aqueous potassium permanganate solution
View Scheme
参考文献
Kruber
Chemische Berichte, 1937 , vol. 70, p. 1556,1563
