Α,Α'-二羟基-1,3-二异丙基苯合成路线 (共 8 条)
反应条件
hydrogen; 5 Pd-CaCO3 in isobutyl methylketone T=98°C; P=3750.38 Torr; 1 h; Conversion of starting material;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2007/197838 A1, 2007 ;
Location in patent: Page/Page column 3-4 ;
反应条件
sodium hydroxide in water; isobutyl methylketone T=90°C; Heating / reflux;
参考文献
US6350921 B1, ;
Example 3 ;
反应条件
sodium hydroxide; 3-isopropyl-1-(2-hydroperoxy-2-propyl)benzene in water T=90°C;
参考文献
US6350921 B1, ;
Example 1 ;
反应条件
sodium hydroxide; oxygen
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 336 - 338
Zhurnal Organicheskoi Khimii, , vol. 22, # 2 p. 381 - 383
反应条件
sodium sulfite in water; isobutyl methylketone Heating / reflux;
参考文献
US6350921 B1, ;
Example 2 ;
反应条件
oxygen; 1,10-phenanthroline; magnesium naphthenate T=80 - 120°C; E(act.) for various reaction products formation, other catalyst; Rate constantKineticsThermodynamic data;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 55, # 3 p. 658 - 662,597 - 601
反应条件
sulfuric acid in isobutyl methylketone T=90°C; P=760.051 Torr; 0.666667 h; Product distribution / selectivity;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2007/197838 A1, 2007 ;
Location in patent: Page/Page column 4 ;
参考文献
Honshu Chemical Industry Co. Ltd.
Patent: US6326522 B1, 2001 ;