1-(三甲基硅氧基)环戊烯合成路线 （共 155 条）
反应条件
Pd/SiO2 in N,N-dimethyl-formamide T=59.9°C; 24 h; various solvents, various reagents; Product distribution;
参考文献
Baba, T.; Nakano, K.; Nishiyama, S.; Tsurya, S.; Masai, M.
Journal of the Chemical Society, Chemical Communications, 1990 , # 4 p. 348 - 349
反应条件
titanium tetrachloride in dichloromethane T=-50°C; 1.5 h;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Chatziiosifidis, Ioannis; Giannis, Athanassios; Heimbach, Horst; Loewe, Ursula
Chemische Berichte, 1980 , vol. 113, # 12 p. 3741 - 3757
反应条件
zinc(II) iodide in dichloromethane 4 h; Ambient temperature;
参考文献
Reetz, M. T.; Huettenhain, S.; Huebner, F.
Synthetic Communications, 1981 , vol. 11, # 3 p. 217 - 222
反应条件
[Ph3SnF2][NBu4] in tetrahydrofuran T=20°C; 6 h;
参考文献
Gingras, Marc
Tetrahedron Letters, 1991 , vol. 32, # 50 p. 7381 - 7384
反应条件
antimony trichloride in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5099 - 5102
反应条件
tetraphosphorus decasulfide T=50 - 60°C; 4 h; Yield given;
参考文献
Nizamov, Il'yas; Kuznetzov, Vladislav A.; Batyeva, Elvira S.; Al'Fonsov, Vladimir A.; Pudovik, Arkady N.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 79, # 1,4 p. 179 - 186
反应条件
boron trifluoride diethyl etherate 1.) methylene dichloride, 20 deg C, 1 h; 2.) 1 h, 20 deg C; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, # 8 p. 1390 - 1395
Zhurnal Organicheskoi Khimii, , vol. 18, # 8 p. 1588 - 1595
反应条件
sulfuryl dichloride in dichloromethane 1) -78 deg C, 2) RT, 30 min;
参考文献
Olah, George A.; Ohannesian, Lena; Arvanaghi, Massoud; Prakash, G. K. Surya
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2032 - 2034
反应条件
N-chloro-succinimide in dichloromethane Heating;
参考文献
Tetrahedron Letters, , vol. 27, # 23 p. 2563 - 2566
反应条件
in dichloromethane Heating;
参考文献
Tetrahedron Letters, , vol. 27, # 23 p. 2563 - 2566
