2-(甲基磺酰基)苯甲酸甲酯合成路线 （共 5 条）
反应条件
3-chloro-benzenecarboperoxoic acid in 1,4-dioxane; water T=20°C; 4 h;
参考文献
NOVARTIS AG; NOVARTIS PHARMA GmbH
Patent: WO2007/67613 A1, 2007 ;
Location in patent: Page/Page column 53-54 ;
WO 2007/067613 A1
反应条件
tetrabutylammomium bromide in water; acetone; toluene T=85°C; 24 h;
参考文献
Sandrinelli, Franck; Perrio, Stephane; Beslin, Pierre
Organic Letters, 1999 , vol. 1, # 8 p. 1177 - 1180
反应条件
1: 100 percent / MeLi; (+/-)-trans-2-(phenylsulfonyl)-3-phenyloxaziridine / tetrahydrofuran; diethyl ether / -78 - -10 °C 2: 77 percent / tetrabutylammonium bromide / H2O; toluene; acetone / 24 h / 85 °C View Scheme
参考文献
Sandrinelli, Franck; Perrio, Stephane; Beslin, Pierre
Organic Letters, 1999 , vol. 1, # 8 p. 1177 - 1180
反应条件
dihydrogen peroxide; Mg-Al-LDH-WO4 T=20°C; 3 h;
参考文献
Choudary; Bharathi; Venkat Reddy; Lakshmi Kantam
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 18 p. 2069 - 2074
反应条件
lithium borohydride in tetrahydrofuran
T=20 - 65°C; 14.75 h;
参考文献
NOVARTIS AG; NOVARTIS PHARMA GmbH
Patent: WO2007/67613 A1, 2007 ;
Location in patent: Page/Page column 54 ;
WO 2007/067613 A1
