1,2-乙烷二基二{二[3,5-二(三氟甲基)苯基]膦}合成路线 (共 4 条)
反应条件
magnesium in diethyl ether T=20°C; 24 h;
参考文献
Wursche, Roland; Debaerdemaeker, Tony; Klinga, Martti; Rieger, Bernhard
European Journal of Inorganic Chemistry, 2000 , # 9 p. 2063 - 2070
反应条件
potassium tert-butylate in tetrahydrofuran 4 h; Heating;
参考文献
Casey, Charles P.; Lin Paulsen, Evelyn; Beuttenmueller, Eckart W.; Proft, Bernd R.; Petrovich, Lori M.; Matter, Brock A.; Powell, Douglas R.
Journal of the American Chemical Society, 1997 , vol. 119, # 49 p. 11817 - 11825
反应条件
1: 77 percent / LiAlH4 / diethyl ether / 2 h / Heating 2: 47 percent / benzene / 20 h / Heating 3: 52 percent / KO-t-Bu / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Casey, Charles P.; Lin Paulsen, Evelyn; Beuttenmueller, Eckart W.; Proft, Bernd R.; Petrovich, Lori M.; Matter, Brock A.; Powell, Douglas R.
Journal of the American Chemical Society, 1997 , vol. 119, # 49 p. 11817 - 11825
反应条件
1: 47 percent / benzene / 20 h / Heating 2: 52 percent / KO-t-Bu / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Casey, Charles P.; Lin Paulsen, Evelyn; Beuttenmueller, Eckart W.; Proft, Bernd R.; Petrovich, Lori M.; Matter, Brock A.; Powell, Douglas R.
Journal of the American Chemical Society, 1997 , vol. 119, # 49 p. 11817 - 11825