in tetrahydrofuran refluxed in THF for 2h; isolated, elem. anal. (impurified with K2(Si(C6H4(O)2)3));
参考文献
Cerveau, Genevieve; Chuit, Claude; Corriu, Robert J. P.; Gerbier, Laurent; Reye, Catherine
Comptes Rendus de l'Academie des Sciences, Serie II: Mecanique, Physique, Chimie, Sciences de la Terre et de l'Univers, 1991 , vol. 312, p. 1311 - 1316
in tetrahydrofuran byproducts: I(1-), H2; under Ar; Fe-complex in soln. added dropwise to a soln. of the Si-compound at 0°C, mixt. stirred for 1 h; solvent removed in vacuo; recrystn. (hexane); IR;
