4-[(甲基磺酰基)氧基]哌啶-1-羧酸苄酯合成路线 (共 8 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Dr. Reddy's Laboratories Ltd.
Patent: EP981526 B1, 2004 ;
Location in patent: Page 20 ;
反应条件
1: triethylamine 2: triethylamine / dichloromethane / 0 °C View Scheme
参考文献
Zhersh, Sergey; Buryanov, Volodymyr V.; Karpenko, Oleksandr V.; Grygorenko, Oleksandr O.; Tolmachev, Andrey A.
Synthesis, 2011 , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: triethylamine 2: triethylamine / dichloromethane / 0 °C View Scheme
参考文献
Zhersh, Sergey; Buryanov, Volodymyr V.; Karpenko, Oleksandr V.; Grygorenko, Oleksandr O.; Tolmachev, Andrey A.
Synthesis, 2011 , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
potassium carbonate in N,N-dimethyl-formamide T=10 - 80°C;
参考文献
Zhersh, Sergey; Buryanov, Volodymyr V.; Karpenko, Oleksandr V.; Grygorenko, Oleksandr O.; Tolmachev, Andrey A.
Synthesis, 2011 , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
triethylamine 72 h; Reflux;
参考文献
PFIZER INC.; NINKOVIC, Sacha; BRAGANZA, John Frederick; COLLINS, Michael Raymond; KATH, John Charles; LI, Hui; RICHTER, Daniel Tyler
Patent: WO2010/16005 A1, 2010 ;
Location in patent: Page/Page column 126-127 ;
WO 2010/016005 A1
反应条件
potassium carbonate in N,N-dimethyl-formamide T=10 - 80°C;
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C 2: water; chlorine / dichloromethane / 0 - 10 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
TBA-CN in dimethyl sulfoxide T=65°C;
参考文献
Winkler, Margit; Meischler, Dorith; Klempier, Norbert
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 8-9 p. 1475 - 1480