甲基(4E)-5,9-二甲基癸-4,8-二烯酸酯合成路线 (共 5 条)
反应条件
in water; N,N-dimethyl-formamide T=160°C; 0.333333 h; microwave irradiation;
参考文献
Curran, Dennis P.; Zhang, Qisheng
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 3 p. 329 - 332
反应条件
1: NaOEt / ethanol / 1 h / -20 °C 2: KOH / methanol 3: 130 °C 4: 10 g / HCl / Heating View Scheme
参考文献
Dyer, Ulrich C.; Robinson, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 53 - 60
反应条件
1: PBr3 / tetrahydrofuran / 0.5 h / 0 °C 2: NaOEt / ethanol / 1 h / -20 °C 3: KOH / methanol 4: 130 °C 5: 10 g / HCl / Heating View Scheme
参考文献
Nakano, Shin-Ichi; Ohashi, Shumi; Hoshino, Tsutomu
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 14 p. 2012 - 2022
反应条件
1: 130 °C 2: 10 g / HCl / Heating View Scheme
参考文献
Nakano, Shin-Ichi; Ohashi, Shumi; Hoshino, Tsutomu
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 14 p. 2012 - 2022
反应条件
hydrogenchloride Heating;
参考文献
Nakano, Shin-Ichi; Ohashi, Shumi; Hoshino, Tsutomu
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 14 p. 2012 - 2022