5-乙酰氨基-6-氨基-3-甲基尿嘧啶(AAMU)合成路线 （共 5 条）
反应条件
1: 95 percent / aq. NaOAc, AcOH, NaNO2 / 0.5 h / 100 °C 2: 82 percent / H2, NaOH / 10percent Pd/C / methanol; H2O / 20 °C / 2625.2 Torr 3: 97 percent / NaOAc, glacial AcOH / 3 h / Heating View Scheme
参考文献
Roehrkasten; Raatz; Kreher; Blaszkewicz
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1997 , vol. 52, # 12 p. 1526 - 1532
反应条件
1: 91 percent / 1N aq. NaOH / 2 h / Heating 2: 95 percent / aq. NaOAc, AcOH, NaNO2 / 0.5 h / 100 °C 3: 82 percent / H2, NaOH / 10percent Pd/C / methanol; H2O / 20 °C / 2625.2 Torr 4: 97 percent / NaOAc, glacial AcOH / 3 h / Heating View Scheme
参考文献
Roehrkasten; Raatz; Kreher; Blaszkewicz
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1997 , vol. 52, # 12 p. 1526 - 1532
反应条件
1: 82 percent / H2, NaOH / 10percent Pd/C / methanol; H2O / 20 °C / 2625.2 Torr 2: 97 percent / NaOAc, glacial AcOH / 3 h / Heating View Scheme
参考文献
Roehrkasten; Raatz; Kreher; Blaszkewicz
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1997 , vol. 52, # 12 p. 1526 - 1532
反应条件
sodium acetate; acetic acid 3 h; Heating;
参考文献
Roehrkasten; Raatz; Kreher; Blaszkewicz
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1997 , vol. 52, # 12 p. 1526 - 1532
反应条件
palladium on activated charcoal; hydrogen
参考文献
Gala; DiBenedetto; Gloor; Jenkins; Kugelman; Maloney; Miller
Organic Process Research and Development, 2004 , vol. 8, # 3 p. 396 - 400
