1-金刚烷-1-基-丙-2-酮合成路线 （共 19 条）
反应条件
1: With InI3 in 1,2-dichloro-ethane T=83°C; 2 h; Inert atmosphere; 2: With sodium hydrogencarbonate in diethyl ether; water; 1,2-dichloro-ethane
参考文献
Nishimoto, Yoshihiro; Onishi, Yoshiharu; Yasuda, Makoto; Baba, Akio
Angewandte Chemie - International Edition, 2009 , vol. 48, # 48 p. 9131 - 9134
反应条件
copper(I) bromide in diethyl ether T=-5°C; 1 h;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
反应条件
indium(III) chloride; trimethylsilyl bromide in 1,2-dichloro-ethane 2 h; Inert atmosphereReflux; chemoselective reaction;
参考文献
Onishi, Yoshiharu; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Organic Letters, 2011 , vol. 13, # 10 p. 2762 - 2765
反应条件
InI3; trimethylsilyl iodide in 1,2-dichloro-ethane T=83°C; 2 h; Inert atmosphere;
参考文献
Onishi, Yoshiharu; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2011 , vol. 40, # 11 p. 1223 - 1225
反应条件
in tetrahydrofuran 1.16667 h;
参考文献
Henkel, James G.; Hane, Jeffrey T.; Gianutsos, Gerald
Journal of Medicinal Chemistry, 1982 , vol. 25, # 1 p. 51 - 56
反应条件
sodium ethanolate in ethanol 10 h; Heating;
参考文献
Klimochkin, Yu.N.; Tilli, T.S.; Moiseev, I.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1605 - 1606
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1780 - 1781
反应条件
1: iodine / dichloromethane / 0.75 h 2: indium(III) chloride; trimethylsilyl bromide / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux View Scheme
参考文献
Onishi, Yoshiharu; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2011 , vol. 40, # 11 p. 1223 - 1225
反应条件
cuprous halogenide in diethyl ether 1 h; Heating;
参考文献
Grava, I. Ya.; Polis, Ya. Yu.; Lidak, M. Yu.; Liepin'sh, E. E.; Shatts, V. D.; et al.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 679 - 686
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 778 - 786
反应条件
in diethyl ether T=0°C; 0.25 h;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
反应条件
sulfuric acid T=10 - 15°C; 3 h;
参考文献
Klimochkin, Yu. N.; Moiseev, I. K.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 1 p. 171 - 172
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 1 p. 207 - 208
