苯基{4-[(三甲基硅烷基)甲基]苯基}甲酮合成路线 (共 4 条)
反应条件
aluminium trichloride in carbon disulfide T=0 - 5°C; Friedel-Crafts acylation; 2 h;
参考文献
Georgakilas, Vasilios; Perdikomatis, Gerasimos P.; Triantafyllou, Anastasios S.; Siskos, Michael G.; Zarkadis, Antonios K.
Tetrahedron, 2002 , vol. 58, # 12 p. 2441 - 2447
反应条件
B-OMe-9-borabicyclo[3.3.1]nonane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran Heating;
参考文献
Fuerstner, Alois; Seidel, Guenter
Tetrahedron, 1995 , vol. 51, # 41 p. 11165 - 11176
反应条件
1: 4-PhCOC6H4I With N,N,N',N'-tetramethyl-urea; zinc T=80°C; 24 h; 2: (iodomethyl)trimethylsilane With 1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2; N,N,N',N'-tetramethyl-urea T=40°C; 24 h;
参考文献
Takahashi, Hideki; Hossain, Kabir M.; Nishihara, Yasushi; Shibata, Takanori; Takagi, Kentaro
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 671 - 675
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; water; caesium carbonate in tetrahydrofuran Suzuki coupling reaction; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo; Ribagorda, Maria; Biolatto, Betina
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5534 - 5539