2,3-二甲基-4-戊烯-2-醇合成路线 (共 14 条)
反应条件
tetra-n-butylammonium perchlorate in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=0°C; electrolysis;
参考文献
Tokuda; Satoh; Suginome
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5608 - 5613
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; tetra-n-butylammonium perchlorate T=0°C; current density = 25 mA/cm2, 2.0 F/mol of halide;
参考文献
Satoh; Suginome; Tokuda
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1791 - 1794
反应条件
ammonium chloride; zinc in water T=25°C;
参考文献
Pasto, Daniel J.; L'Hermine, Gael
Tetrahedron, 1993 , vol. 49, # 16 p. 3259 - 3272
反应条件
in N,N-dimethyl-formamide T=0 - 30°C; cathodic reduction;
参考文献
Sibille, Soline; d'Incan, Esther; Leport, Louis; Perichon, Jacques
Tetrahedron Letters, 1986 , vol. 27, # 27 p. 3129 - 3132
反应条件
in diethyl ether T=-5°C;
参考文献
Ashcroft, Martyn R.; Bury, Adrian; Cooksey, Christopher J.; Davies, Alwyn G.; Gupta, B. Dass; et al.
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 89 - 104
反应条件
in N,N-dimethyl-formamide T=0 - 30°C; cathodic reduction;
参考文献
Sibille, Soline; d'Incan, Esther; Leport, Louis; Perichon, Jacques
Tetrahedron Letters, 1986 , vol. 27, # 27 p. 3129 - 3132
参考文献
Klei, Bert; Teuben, Jan H.; Meijer, Henk J. de Liefde
Journal of the Chemical Society, Chemical Communications, 1981 , # 7 p. 342 - 344
反应条件
chromium sulphate in N,N-dimethyl-formamide
参考文献
Zurqiyah,A.; Castro,C.E.
Journal of Organic Chemistry, 1969 , vol. 34, p. 1504 - 1506
反应条件
(i) pentane, (ii) H2NCH2CH2OH; Multistep reaction;
参考文献
Kramer,G.W.; Brown,H.C.
Journal of Organic Chemistry, 1977 , vol. 42, p. 2292 - 2299
反应条件
(i), (ii) (HOCH2CH2)3N; Multistep reaction;
参考文献
Mikhailov,B.M. et al.
Journal of Organometallic Chemistry, 1978 , vol. 154, p. 131 - 145