D,L-色氨酸甲酯苯并醛亚胺合成路线 (共 5 条)
反应条件
in benzene 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 49, # 15 p. 2699 - 2701
反应条件
1: tryptophane methyl ester hydrochloride With magnesium sulfate; triethylamine in dichloromethane T=20°C; 1 h; 2: benzaldehyde in dichloromethane T=20°C;
参考文献
Chemical Communications, , # 20 p. 2905 - 2907
反应条件
benzoic acid in benzene 48 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 185 - 187
反应条件
1: H2 / platinum oxide / methanol 2: NaOH / methanol; H2O / 2 h / Heating View Scheme
参考文献
Baggaley, Keith H.; Fears, Robin; Ferres, Harry; Geen, Graham R.; Hatton, Ian K.; et al.
European Journal of Medicinal Chemistry, 1988 , vol. 23, p. 523 - 532
反应条件
1: 1.) LDA / 1.) THF, -78 deg C, 0.5 h, 2.) THF, RT, overnight 2: 1N aq. HCl / 1 h / Ambient temperature View Scheme
参考文献
Brana, Miguel F.; Garrido, Mercedes; Rodriguez, Maria L. Lopez; Morcillo, M. Jose
Heterocycles, 1987 , vol. 26, # 8 p. 2139 - 2151