in dichloromethane 1 h; Ambient temperature; Yield given;

in chloroform T=23°C;

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1696894', constants.ctx, '0')">diethyl ether</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=-30&deg;C;&nbsp;0.166667&nbsp;h;&nbsp;<br /> &nbsp;