反应条件
1.1: hydrogen / ethanol / 6.5 h / 25 - 70 °C / 3878.71 - 7757.43 Torr / |Large scale 2.1: acetic acid; palladium 10 on activated carbon; hydrogen / toluene; water; ethanol / 8 h / 20 - 25 °C / 7757.43 Torr / |Large scale 2.2: 20 °C / |Large scale 3.1: pyridine / toluene / 100 - 110 °C / |Large scale 3.2: 106 - 110 °C / |Large scale 4.1: lithium tert-butylate / toluene; hexane / -10 °C / |Large scale View Scheme
参考文献
Storace, Louis; Anzalone, Luigi; Confalone, Pat N.; Davis, Wayne P.; Fortunak, Joseph M.; Giangiordano, Mark; Haley Jr., James J.; Kamholz, Kenneth; Li, Hui-Yin; Ma, Philip; Nugent, William A.; Parsons Jr., Rodney L.; Sheeran, Patrick J.; Silverman, Charlotte E.; Waltermire, Robert E.; Wood, Christopher C.
Organic Process Research and Development, 2002 , vol. 6, # 1 p. 54 - 63
