Boc-S-乙酰氨甲基-L-半胱氨酸合成路线 (共 12 条)
反应条件
TMG in N,N-dimethyl-formamide
参考文献
Journal of the American Chemical Society, , vol. 94, # 15 p. 5456 - 5461
参考文献
Tetrahedron letters, , vol. 26, p. 3057 - 3058
参考文献
Chemistry of Natural Compounds, , vol. 15, p. 471 - 476
Khimiya Prirodnykh Soedinenii, , vol. 15, p. 543 - 548
反应条件
methyltrichloromonosilane; bis-(phenyl)-sulfoxide; trifluoroacetic acid T=4°C; 0.166667 h; var. reaction times, silyl chlorides and sulfoxides; other S-protected cystine-peptides; Product distributionMechanism;
参考文献
Akaji, Kenichi; Tatsumi, Tadashi; Yoshida, Makoto; Kimura, Tooru; Fujiwara, Yoichi; Kiso, Voshiaki
Journal of the American Chemical Society, 1992 , vol. 114, # 11 p. 4137 - 4143
反应条件
silver tetrafluoroborate; methoxybenzene in trifluoroacetic acid T=4°C; 1 h;
参考文献
Yoshida; Tatsumi; Fujiwara; Iinuma; Kimura; Aka ji; Kiso
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 6 p. 1551 - 1557
反应条件
silver tetrafluoroborate; methoxybenzene in trifluoroacetic acid
参考文献
Yoshida; Akaji; Tatsumi; Iinuma; Fujiwara; Kimura; Kiso
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 1 p. 273 - 275
反应条件
in acetic acid T=0°C; 0.5 h;
参考文献
Matsueda, Rei; Higashida, Susumu; Ridge, Richard J.; Matsueda, Gary R.
Chemistry Letters, 1982 , p. 921 - 924
参考文献
Fauchere, Jean-Luc; Pliska, Vladimir
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 4 p. 369 - 376
反应条件
methyltrichloromonosilane; bis-(phenyl)-sulfoxide; trifluoroacetic acid T=4°C; 0.166667 h; var. reaction times, silyl chlorides and sulfoxides; other S-protected cystine-peptides; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 114, # 11 p. 4137 - 4143
反应条件
N-bromosuccinmide; trifluoroacetic acid multistep reaction; other cysteine derivatives; other solvent and reaction time; other N-halosuccinimides; conversion of cysteine derivatives into cystine by N-halosuccinimides;
参考文献
Shih, Hsiencheng
Journal of Organic Chemistry, 1993 , vol. 58, # 11 p. 3003 - 3008