3,3’-二氯二苯二硫醚合成路线 （共 13 条）
反应条件
silica supported cobalt(II) tetrasulfophthalocyanine in ethyl acetate T=20°C; 1.5 h;
参考文献
Bayraq, Samad Shoghpour; Nikseresht, Ahmad; Khosravi, Iman
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 9 p. 1236 - 1243
反应条件
PPA; Polyphosphoric acid (PPA) in chlorobenzene 3.75 h; Heating / reflux;
参考文献
US2004/6229 A1, ;
Page/Page column 38 ;
US 20040006229 A1
反应条件
[BnEt3N]2MoS4 in acetonitrile T=0 - 25°C; 8 h;
参考文献
Bhar; Chandrasekaran
Synthesis, 1994 , # 8 p. 785 - 786
反应条件
hydrogenchloride; sodium sulfide; oxygen in water T=20°C; 2.5 h;
参考文献
European Journal of Inorganic Chemistry, , # 30 p. 4801 - 4810
反应条件
1.1: sulfuric acid; sodium nitrite / 20 °C 1.2: 20 °C 2.1: hydrogenchloride; sodium sulfide; oxygen / water / 2.5 h / 20 °C View Scheme
参考文献
European Journal of Inorganic Chemistry, , # 30 p. 4801 - 4810
反应条件
phosphorus; hydrogen bromide in acetic acid
参考文献
Australian Journal of Chemistry, , vol. 26, p. 121 - 134
反应条件
zinc in ethylene glycol dimethyl ether 48 h; Title compound not separated from byproducts;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 35, p. 375 - 386
反应条件
ammonium cerium(IV) nitrate in water; acetic acid T=25 - 45°C; ΔH(excit.), ΔS(excit.); KineticsThermodynamic data;
参考文献
Tetrahedron, , vol. 50, # 48 p. 13731 - 13738
反应条件
in 1,4-dioxane T=120°C; Kinetics;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 185, # 5-6 p. 1162 - 1173
反应条件
in water; tert-butyl alcohol T=30°C; Rate constant;
参考文献
Happer,D.A.R. et al.
Australian Journal of Chemistry, 1973 , vol. 26, p. 121 - 134
