4'-苯甲酰基苯甲酰苯胺合成路线 (共 20 条)
反应条件
pyridine in dichloromethane T=20°C; 3 h;
参考文献
Dannhardt, Gerd; Fiebich, Bernd L; Schweppenhaeuser, Johannes
European Journal of Medicinal Chemistry, 2002 , vol. 37, # 2 p. 147 - 161
反应条件
1: (4-Amino-phenyl)phenyl-methanone With lithium diisopropyl amide in hexane T=20°C; 1 h; 2: benzoyl-protected allyl alcohol in hexane T=0 - 20°C;
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
cyclohexa-1,4-diene in benzene T=20°C; 0.5 h; UV-irradiationInert atmosphere;
参考文献
Chowdhury, Nilanjana; Dutta, Sansa; Nishitha, Boda; Dasgupta, Swagata; Singh, N.D. Pradeep
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 18 p. 5414 - 5417
反应条件
1: With methanesulfonic acid; phosphorous pentoxide T=80 - 110°C; Fries rearrangement; 2: With sodium hydroxide in water
参考文献
Kaboudin, Babak; Abedi, Yaghoub
Organic Preparations and Procedures International, 2009 , vol. 41, # 3 p. 229 - 236
反应条件
1.1: 87 percent / thionyl chloride / 0 - 20 °C 2.1: lithium diisopropylamine / hexane / 1 h / 20 °C 2.2: 58 percent / hexane / 0 - 20 °C View Scheme
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
in methanol T=20°C; 0.166667 h; Inert atmosphereUV-irradiation;
参考文献
Chowdhury, Nilanjana; Dutta, Sansa; Nishitha, Boda; Dasgupta, Swagata; Singh, N.D. Pradeep
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 18 p. 5414 - 5417
反应条件
aluminium trichloride 1.) 1,2-dichloroethane, 0-5 deg C, 15 min., 2.) 5 h; Yield given. Multistep reaction;
参考文献
Ayyanger; Lahoti; Srinivasan; Daniel
Synthesis, 1991 , # 4 p. 322 - 324
反应条件
2: zinc chloride / 180 °C / Kochen des Produkts mit alkoh. Kali View Scheme
参考文献
Doebner
Justus Liebigs Annalen der Chemie, 1881 , vol. 210, p. 267
反应条件
1: zinc chloride / 180 °C / Kochen des Produkts mit alkoh. Kali View Scheme
参考文献
Doebner
Justus Liebigs Annalen der Chemie, 1881 , vol. 210, p. 267
反应条件
1: zinc chloride / 180 °C / Kochen des Produkts mit alkoh. Kali View Scheme
参考文献
Doebner
Justus Liebigs Annalen der Chemie, 1881 , vol. 210, p. 267