(±)-3-羟基十四烷酸合成路线 （共 17 条）
反应条件
1,4-dioxane; methanol; nickel T=100°C; P=73550.8 Torr; Hydrogenation.und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge;
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 6, p. 809,812
反应条件
P450BSβ enzyme; cadmium(II) sulphide in ethanol T=20°C; 0.333333 h; Irradiation; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 3 p. 504 - 507
反应条件
sodium hydroxide in methanol Ambient temperature; Yield given;
参考文献
Arzneimittel-Forschung/Drug Research, , vol. 39, # 10 p. 1190 - 1195
反应条件
1: pyridine / CH2Cl2 / 0 deg C, 1 h then r.t., 4 h 2: 3 h / Heating 3: NaBH4 / methanol / 2 h / 5 - 10 °C 4: NaOH / methanol / Ambient temperature View Scheme
参考文献
Arzneimittel-Forschung/Drug Research, , vol. 39, # 10 p. 1190 - 1195
反应条件
1: 3 h / Heating 2: NaBH4 / methanol / 2 h / 5 - 10 °C 3: NaOH / methanol / Ambient temperature View Scheme
参考文献
Arzneimittel-Forschung/Drug Research, , vol. 39, # 10 p. 1190 - 1195
反应条件
sodium chlorite; potassium dihydrogenphosphate Oxidation;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 18 p. 2107 - 2110
反应条件
1: 84 percent / TiCl4 2: OsO4; NMO 3: NaIO4 4: NaClO2; KH2PO4 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 18 p. 2107 - 2110
反应条件
1: OsO4; NMO 2: NaIO4 3: NaClO2; KH2PO4 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 18 p. 2107 - 2110
反应条件
potassium hydroxide; zinc 1.) benzene, reflux, 7 h, 2.) MeOH, room temperature; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 19, # 11-12 p. 2035 - 2040
反应条件
potassium hydroxide; ethanol 40 h; Ambient temperature; Yield given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 875 - 880
