N-(1-羟基-2,2,2-三氟乙亚基)-叔-丁胺合成路线 (共 7 条)
反应条件
triethylamine; trichloroacetonitrile; triphenylphosphine in acetonitrile T=20°C; 3 h; Inert atmosphere;
参考文献
Kim, Joong-Gon; Jang, Doo Ok
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 683 - 685
参考文献
Steffel, Lauren R.; Cashman, Timothy J.; Reutershan, Michael H.; Linton, Brian R.
Journal of the American Chemical Society, 2007 , vol. 129, # 43 p. 12956 - 12957
反应条件
in tetrahydrofuran 48 h; Ambient temperature;
参考文献
Svirskaya, Polina I.; Leznoff, Clifford C.; Steinman, Martin
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1362 - 1364
反应条件
in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Katritzky, Alan R.; Yang, Baozhen; Semenzin, Delphine
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 726 - 728
反应条件
pyridine in dichloromethane T=-50°C; Yield given;
参考文献
Froyen, Paul
Tetrahedron Letters, 1997 , vol. 38, # 30 p. 5359 - 5362
反应条件
in tetrahydrofuran 12 h; Heating;
参考文献
Katritzky, Alan R.; Yang, Baozhen; Guofang, Qiu; Zhang, Zhongxing
Synthesis, 1999 , # 1 p. 55 - 57
反应条件
sodium hydroxide; potassium carbonate in acetonitrile T=25°C; 3 h;
参考文献
Albanese; Penso
Synthesis, 1991 , # 11 p. 1001 - 1002