1.1: dichloromethane / 12 h / 20 °C 2.1: triethylamine / dichloromethane / 96 h / |Reflux 3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C 3.2: 3 h / 20 °C 4.1: Grubb's 2nd generation catalyst / dichloromethane / 2 h / 45 °C / |Inert atmosphere; |Sealed tube 5.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C View Scheme

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1: 4.6 percent / CuCl2, triethylaminium halide / benzene / 40 °C 2: 89 percent / triethylamine / benzene / 0.25 h / Ambient temperature View Scheme

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