反应条件
1: 0.93 M DIBALH-hexane / CH2Cl2; 1,2-dimethoxy-ethane / 0.75 h / -78 °C
2: tetrahydrofuran; diethyl ether / 8 h / Ambient temperature
3: PCC, 4-A molecular sieves / 1 h / Ambient temperature
View Scheme
参考文献
Ihara, Masataka; Taniguchi, Takahiko; Makita, Kei; Takano, Michiko; Ohnishi, Masaru; Taniguchi, Nobuaki; Fukumoto, Keiichiro; Kabuto, Chizuko
Journal of the American Chemical Society, 1993 , vol. 115, # 18 p. 8107 - 8115