2,2'-亚甲基双苯并噻唑合成路线 (共 11 条)
反应条件
n-butyl-magnesium bromide in tetrahydrofuran 8 h; Heating;
参考文献
Babudri, Francesco; Florio, Saverio; Ingrosso, Giovanni; Turco, Anna Maria
Heterocycles, 1986 , vol. 24, # 8 p. 2215 - 2218
反应条件
PPA T=125 - 150°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 26, p. 3434 - 3436
反应条件
PPA 1.) 80-90 deg C, 2 h; 2.) 120 deg C, 3 h; 3.) 140 deg C, 1 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 247 - 249
反应条件
in toluene 24 h; Heating;
参考文献
Canadian Journal of Chemistry, , vol. 66, p. 2339 - 2344
反应条件
in ethanol 48 h; Reflux;
参考文献
Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 11 p. 2856 - 2869
参考文献
Journal of the Chemical Society, , vol. 121, p. 464
反应条件
air; triethylamine in dimethyl sulfoxide 12 h; Ambient temperature;
参考文献
Boga, Carla; Forlani, Luciano; Todesco, Paolo E.
Gazzetta Chimica Italiana, 1997 , vol. 127, # 4 p. 197 - 200
反应条件
potassium dichromate; sulfuric acid in acetic acid 2 h; Ambient temperaturevar. temp.:65-75 deg C; var. reag.: CrO3, Mn(OAc)2, Pb(OAc)2*3H2O, Fe(OAc)2, NaOMe in MeOH in air; Product distribution;
参考文献
Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Gazzetta Chimica Italiana, 1996 , vol. 126, # 6 p. 329 - 338
反应条件
potassium permanganate; sulfuric acid in acetic acid 2 h; Ambient temperature;
参考文献
Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Gazzetta Chimica Italiana, 1996 , vol. 126, # 6 p. 329 - 338
反应条件
potassium dichromate; sulfuric acid in acetic acid 2 h; Ambient temperaturevar. temp.:65-75 deg C; var. reag.: CrO3, Mn(OAc)2, Pb(OAc)2*3H2O, Fe(OAc)2, NaOMe in MeOH in air; Product distribution;
参考文献
Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Gazzetta Chimica Italiana, 1996 , vol. 126, # 6 p. 329 - 338