1-氯六氢-2H-氮杂卓-2-酮合成路线 （共 6 条）
反应条件
sodium hypochlorite; acetic acid; tert-butyl alcohol in toluene T=0°C; 2 h;
参考文献
MERCK and CO., INC.
Patent: WO2006/60225 A2, 2006 ;
Location in patent: Page/Page column 36; 38 ;
参考文献
Caprara et al.
Annali di Chimica (Rome, Italy), 1959 , vol. 49, p. 1167,1171
反应条件
1: N-chloro-ε-caprolactam in dichloromethane T=-78°C; Photolysis; 2: methanol With triethylamine in dichloromethane T=20°C; 2 h;
参考文献
Drouin, Alexandre; Lessard, Jean
Tetrahedron Letters, 2006 , vol. 47, # 25 p. 4285 - 4288
反应条件
0.25 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 48, # 26 p. 5164 - 5170
反应条件
1: N-chloro-ε-caprolactam in dichloromethane
T=-78°C; Photolysis;
2: methanol With triethylamine in dichloromethane
T=20°C; 2 h;
参考文献
Drouin, Alexandre; Lessard, Jean
Tetrahedron Letters, 2006 , vol. 47, # 25 p. 4285 - 4288
反应条件
0.25 h; Irradiation;
参考文献
Phan, Xuan T.; Shannon, Paul J.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5164 - 5170
