1-硝基-4-苯基乙炔苯合成路线 （共 107 条）
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in water
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide
T=80°C; sila-Sonogashira reaction; 3 h;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
反应条件
copper(l) iodide; triethylamine; Titanium(IV) oxide
T=20°C; 24 h;
参考文献
Li, Jin-Heng; Liang, Yun; Xie, Ye-Xiang
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4393 - 4396
反应条件
pyrrolidine; montmorillonite K-10; [PdBr(CNC-Me2)]Br
T=87°C; Sonogashira coupling; 0.5 h;
参考文献
Lin, Bo-Nan; Huang, Shao-Hsien; Wu, Wei-Yi; Mou, Chung-Yuan; Tsai, Fu-Yu
Molecules, 2010 , vol. 15, # 12 p. 9157 - 9173
反应条件
palladium 10 on activated carbon; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl acetamide
T=110°C; Sonogashira coupling; 2 h; Inert atmosphere;
参考文献
Komaromi, Anna; Novak, Zoltan
Chemical Communications, 2008 , # 40 p. 4968 - 4970
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran; acetonitrile
T=25°C; Sonogashira coupling; 1.5 h; Inert atmosphere;
参考文献
Man, Wing Y.; Bock, Soeren; Zaitseva, Natasha N.; Bruce, Michael I.; Low, Paul J.
Journal of Organometallic Chemistry, 2011 , vol. 696, # 10 p. 2172 - 2176
反应条件
potassium phosphate; copper(l) iodide; 8-hydroxy-quinoline in ethanol
T=100°C; Suzuki Coupling; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Liu, Jidan; Dai, Fenglin; Yang, Zhiyong; Wang, Sizhuo; Xie, Kai; Wang, Anwei; Chen, Xiang; Tan, Ze
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5678 - 5683
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=20°C; Hiyama Coupling; 12 h;
参考文献
Tang, Jiansheng; Guo, Cancheng
Journal of Chemical Research, 2014 , vol. 38, # 2 p. 123 - 127
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=20°C; Hiyama Coupling; 12 h;
参考文献
Tang, Jiansheng; Guo, Cancheng
Journal of Chemical Research, 2014 , vol. 38, # 2 p. 123 - 127
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; palladium diacetate in 1,4-dioxane
T=100°C; Stille reaction; 16 h;
参考文献
Li, Jin-Heng; Liang, Yun; Wang, De-Ping; Liu, Wen-Jie; Xie, Ye-Xiang; Yin, Du-Lin
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2832 - 2834
