1-硝基-4-苯基乙炔苯合成路线 (共 107 条)
反应条件
chlorobenzene in dichloromethane
T=120 - 130°C; P=0.001 Torr; 3 h; solvent-dichloroethane, 1.5h; Product distribution;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 3 p. 411 - 417
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 3 p. 457 - 464
反应条件
(4-nitrophenyl)Pd(P(C6H5)3)2I in dichloromethane
T=120 - 130°C; P=0.001 Torr; 1.5 h; Product distribution;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 3 p. 411 - 417
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 3 p. 457 - 464
反应条件
acetic acid; sodium nitrite
1 h; Ambient temperature;
参考文献
Beccalli, Egle M.; Manfredi, Amedea; Marchesini, Alessandro
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2372 - 2375
反应条件
1: acetone; CuCl2; CaO
2: KOH; dioxane
View Scheme
参考文献
Dombrowskii; Jurkewitsch; Terent'ew
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 3047,3049
J. Gen. Chem. USSR (Engl. Transl.), 1957 , vol. 27, p. 3077
反应条件
in dichloromethane
T=120 - 130°C; P=0.001 Torr; 2 h; Product distributionMechanism;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 3 p. 411 - 417
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 3 p. 457 - 464
反应条件
Oxonereg;; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; [Ru(cymene)Cl2]2; sodium hydrogencarbonate in nitromethane; water
T=20°C; 12 h;
参考文献
Xu, Yuan; Wan, Xiaobing
Tetrahedron Letters, 2013 , vol. 54, # 7 p. 642 - 645
参考文献
Ye, Chengfeng; Xiao, Ji-Chang; Twamley, Brendan; LaLonde, Aaron D.; Norton, M. Grant; Shreeve, JeaN'Ne M.
European Journal of Organic Chemistry, 2007 , # 30 p. 5095 - 5100