1-硝基-4-苯基乙炔苯合成路线 (共 107 条)
反应条件
quinoline; hydrogen; palladium on barium sulfate in ethanol
参考文献
Journal of Medicinal Chemistry, , vol. 18, # 4 p. 386 - 391
反应条件
oxygen; palladium diacetate; zinc(II) chloride T=100°C; P=5700.38 Torr; 24 h;
参考文献
Wang, Azhong; Jiang, Huanfeng
Journal of the American Chemical Society, 2008 , vol. 130, # 15 p. 5030 - 5031
反应条件
formic acid; triethylamine; palladium on activated charcoal 18 h; Heating;
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
thallous acetate; cesium fluoride; bis(dibenzylideneacetone)-palladium(0) in toluene; acetonitrile T=90°C; 8 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 14 p. 2535 - 2538
反应条件
[Pd((.eta.5-C5H5)Fe[(.eta.5-C5H3)C(Me)=N(C6H4-4-Me)])ClPPh3]; tetrabutylammomium bromide; potassium carbonate; benzoic acid in N,N-dimethyl-formamide T=110°C; 4 h; Inert atmosphere;
参考文献
Zhang, Junli; Yang, Fan; Wu, Yangjie
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 675 - 679
反应条件
(5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride; oxygen in hexane T=150°C; P=15001.5 Torr; 4 h;
参考文献
Sheng, Wen-Bing; Jiang, Qing; Luo, Wei-Ping; Guo, Can-Cheng
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5691 - 5693
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; sodium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=80°C; Larock Annulation; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Phetrak, Nared; Rukkijakan, Thanya; Sirijaraensre, Jakkapan; Prabpai, Samran; Kongsaeree, Palangpon; Klinchan, Chayada; Chuawong, Pitak
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12703 - 12709
反应条件
nickel in N,N-dimethyl-formamide 0.25 h; Ambient temperature;
参考文献
Yasuhara; Kasano; Sakamoto
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2301 - 2303
反应条件
5 Au/Fe2O3; hydrogen in toluene T=60°C; P=15001.5 Torr; 1 h; Autoclave; chemoselective reaction;
参考文献
Organic Letters, , vol. 11, # 22 p. 5162 - 5165
反应条件
diiron nonacarbonyl; tributylphosphine; 4-bromooctafluorobutanetriethoxysilane in tetrahydrofuran T=60°C; 48 h; Inert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Enthaler, Stephan; Haberberger, Michael; Irran, Elisabeth
Chemistry - An Asian Journal, 2011 , vol. 6, # 6 p. 1613 - 1623