2-乙酰氨基-6-氯-苯甲酸合成路线 （共 15 条）
参考文献
Jin, Yi; Li, Hui-Yuan; Lin, Li-Ping; Tan, Jinzhi; Ding, Jian; Luo, Xiaomin; Long, Ya-Qiu
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 19 p. 5613 - 5622
反应条件
1: potassium carbonate; copper; amyl alcohol
2: aqueous H2SO4
View Scheme
参考文献
Goldberg; Kelly
Journal of the Chemical Society, 1946 , p. 102,107
反应条件
1: potassium carbonate; copper; amyl alcohol
2: aqueous H2SO4
3: sodium-amalgam; ethanol; water / anschl. mit FeCl3 und wss. HCl
View Scheme
参考文献
Goldberg; Kelly
Journal of the Chemical Society, 1946 , p. 102,107
反应条件
1: hydrochloric acid / 1.5 h / 80 - 90 °C
2: 67.6 percent / 2 h / 130 - 175 °C
3: 51.6 percent / H2SO4; nitric acid / 0.17 h / 0 °C
View Scheme
参考文献
Jin, Yi; Li, Hui-Yuan; Lin, Li-Ping; Tan, Jinzhi; Ding, Jian; Luo, Xiaomin; Long, Ya-Qiu
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 19 p. 5613 - 5622
反应条件
1: aqueous hydrochloric acid
2: aqueous hydrochloric acid; sodium nitrite / Diazotization.Eintragen der erhaltenen Diazoniumsalz-Loesung in eine aus Kupfer(II)-sulfat, Schwefeldioxid und wss. Ammoniak hergestellte Loesung
View Scheme
参考文献
Huntress; Cliff
Journal of the American Chemical Society, 1933 , vol. 55, p. 2559,2563
