2,4,6-三碘间苯二酚合成路线 (共 16 条)
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate in methanol; dichloromethane 4 h; Ambient temperature;
参考文献
Kajigaeshi, Shoji; Kakinami, Takaaki; Yamasaki, Hiromichi; Fujisaki, Shizuo; Kondo, Manabu; Okamoto, Tsuyoshi
Chemistry Letters, 1987 , p. 2109 - 2112
反应条件
calcium carbonate in methanol; dichloromethane; ethyl acetate
参考文献
Sterling Winthrop Inc.
Patent: US5336484 A1, 1994 ;
反应条件
[K*18-crown-6]ICl2; potassium carbonate in acetonitrile T=25°C; 2 h; regioselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 8 p. 2987 - 2991
反应条件
iodine; sodium hydrogencarbonate in water T=25°C; 20 h;
参考文献
Thomsen, Ib; Torssell, Kurt B. G.
Acta Chemica Scandinavica, 1991 , vol. 45, # 5 p. 539 - 542
反应条件
iodine; sodium hydrogencarbonate in water
参考文献
Greig, Lyndsey M.; Slawin, Alexandra M.Z.; Smith, Melanja H.; Philp, Douglas
Tetrahedron, 2007 , vol. 63, # 11 p. 2391 - 2403
反应条件
1: Kalischmelze 2: water; KI / man macht mit Alkali alkalisch, verduennt setzt Chlorkalkloesung und dann Salzsaeure hinzu View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 20, p. 324
参考文献
Yakugaku Zasshi, , vol. 63, p. 20,24
Chem.Abstr., , p. 7265
Pharmaceutica Acta Helvetiae, , vol. 21, p. 225,227
参考文献
Yakugaku Zasshi, , vol. 63, p. 20,24
Chem.Abstr., , p. 7265
Pharmaceutica Acta Helvetiae, , vol. 21, p. 225,227
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 20, p. 324
参考文献
Chemische Berichte, , vol. 9, p. 1752