二萘并[2,1-b:1',2'-d]噻吩合成路线 (共 15 条)
反应条件
nickel/molybdenum on alumina; hydrogen in decalin T=300°C; P=37998 Torr; 4 h;
参考文献
Staiger, Chad L.; Loy, Douglas A.; Jamison, Gregory M.; Schneider, Duane A.; Cornelius, Christopher J.
Journal of the American Chemical Society, 2003 , vol. 125, # 33 p. 9920 - 9921
反应条件
T=400°C; P=0.1 Torr; 3 h;
参考文献
Staiger, Chad L.; Loy, Douglas A.; Jamison, Gregory M.; Schneider, Duane A.; Cornelius, Christopher J.
Journal of the American Chemical Society, 2003 , vol. 125, # 33 p. 9920 - 9921
反应条件
T=271°C; 0.366667 h;
参考文献
Cossu, Sergio; De Lucchi, Ottorino; Fabbri, Davide; Valle, Giovanni; Painter, Gavin F.; Smith, Robin A.J.
Tetrahedron, 1997 , vol. 53, # 17 p. 6073 - 6084
反应条件
potassium hydroxide; N,N-dimethylthiocarbamoyl chloride
Yield given. Multistep reaction;
参考文献
Cossu, Sergio; Delogu, Giovanna; Lucchi, Ottorino De; Fabbri, Davide; Fois, Maria Paola
Synthetic Communications, 1989 , vol. 19, # 20 p. 3431 - 3436
反应条件
iodine; methyloxirane in cyclohexane
0.5 h; Irradiation;
参考文献
Sadorn, Karoon; Sinananwanich, Warapon; Areephong, Jetsuda; Nerungsi, Chakkrapan; Wongma, Chalayut; Pakawatchai, Chaveng; Thongpanchang, Tienthong
Tetrahedron Letters, 2008 , vol. 49, # 29-30 p. 4519 - 4521
反应条件
sodium thiomethoxide in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=100°C; 3 h;
参考文献
Furia, F. di; Licini, G.; Modena, G.; Valle, G.
Bulletin de la Societe Chimique de France, 1990 , # 6 p. 734 - 744
反应条件
in sulfolane
T=285°C; 0.75 h;
参考文献
Furia, F. di; Licini, G.; Modena, G.; Valle, G.
Bulletin de la Societe Chimique de France, 1990 , # 6 p. 734 - 744
反应条件
cyclohexa-1,4-diene in benzene
T=200°C; Bergman cyclization; 4 h;
参考文献
Lewis, Kevin D.; Rowe, Michael P.; Matzger, Adam J.
Tetrahedron, 2004 , vol. 60, # 34 p. 7191 - 7196
反应条件
air; iodine in cyclohexane
Irradiation;
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: sodium hydride / dimethylformamide / 3 h / 90 °C
2: 250 °C
View Scheme
参考文献
Gladiali; Medici; Pirri; Pulacchini; Fabbri
Canadian Journal of Chemistry, 2001 , vol. 79, # 5-6 p. 670 - 678