N-甲基-N-苯基苯甲酰胺合成路线 (共 96 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate; potassium iodide in N,N-dimethyl-formamide
T=120°C; Molecular sieve;
参考文献
Ran, Longfei; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Chemistry - An Asian Journal, 2014 , vol. 9, # 2 p. 577 - 583
反应条件
4,4'-azpy; triphenylphosphine in acetonitrile
Mitsunobu reaction; 5.5 h; Reflux;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Khalili, Dariush
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 8 p. 923 - 934
反应条件
1: iodobenzene; N-methylaniline With sodium carbonate in water
0.166667 h; Autoclave;
2: carbon dioxide in water
T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Qureshi, Ziyauddin S.; Revankar, Santosh A.; Khedkar, Mayur V.; Bhanage, Bhalchandra M.
Catalysis Today, 2012 , vol. 198, # 1 p. 148 - 153
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; ethyl acetate
T=90°C; 24 h; Reagent/catalystSolvent;
参考文献
Wang, Shan; Wang, Jian; Guo, Rui; Wang, Gao; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron Letters, 2013 , vol. 54, # 46 p. 6233 - 6236
反应条件
potassium phosphate; copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione in toluene
T=130°C; 24 h; Inert atmosphere;
参考文献
Racine, Emilie; Monnier, Florian; Vors, Jean-Pierre; Taillefer, Marc
Organic Letters, 2011 , vol. 13, # 11 p. 2818 - 2821
反应条件
1,4-diaza-bicyclo[2.2.2]octane; bicycloheptadienemolybdenunim tetracarbonyl; tetrabutylammomium bromide in diethylene glycol dimethyl ether
T=140°C; 2 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Motevalli, Somayeh; Talebi, Mohsen
Tetrahedron, 2013 , vol. 69, # 1 p. 418 - 426
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; ethyl acetate
T=90°C; 24 h;
参考文献
Wang, Shan; Wang, Jian; Guo, Rui; Wang, Gao; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron Letters, 2013 , vol. 54, # 46 p. 6233 - 6236
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; acetonitrile
T=90°C; 15 h; Reagent/catalystSolvent;
参考文献
Song, Ge; Sun, Gangchun; Tang, Yamin; Mai, Wenpeng
Journal of Chemical Research, 2013 , vol. 37, # 10 p. 630 - 632
反应条件
sodium iodide in dimethyl sulfoxide
T=20°C; Electrochemical reaction;
参考文献
Huang, Haolai; Yuan, Gaoqing; Li, Xianwei; Jiang, Huanfeng
Tetrahedron Letters, 2013 , vol. 54, # 52 p. 7156 - 7159
反应条件
1-methyl-1H-imidazole; N,N,N',N,-tetramethylethylenediamine; potassium carbonate in potassium hydroxide
T=20 - 25°C; Schotten-Baumann-type reaction; pH=11.5; 1.5 h;
参考文献
Zhou, Shaolin; Junge, Kathrin; Addis, Daniele; Das, Shoubhik; Beller, Matthias
Angewandte Chemie - International Edition, 2009 , vol. 48, # 50 p. 9507 - 9510