(1,10-亚铁试剂)二溴铜(II)合成路线 (共 2 条)
反应条件
CuI in water High Pressure; a mixt. of CuI, CuBr2, phenanthroline and H2O in a molar ratio 1:2:1.5:400 was stirred and heated at 160°C for 4 days under autogenous pressure; crystals were filtered, washed with distilled water and dried in air at ambient temp.; elem. anal.;
参考文献
Yu, Jie-Hui; Lue, Zheng-Liang; Xu, Ji-Qing; Bie, Hai-Ying; Lu, Jing; Zhang, Xiao
New Journal of Chemistry, 2004 , vol. 28, # 8 p. 940 - 945
反应条件
in ethanol react. mixt. refluxed, microcryst. solid formed upon cooling; recrystd. from hot dimethylacetamide;
参考文献
Garland, M. T.; Grandjean, D.; Spodine, E.; Atria, A. M.; Manzur, J.
Acta Crystallographica, Section C: Crystal Structure Communications, 1988 , vol. 44, p. 1547 - 1549