4,4-二甲基-2-苯基-2-噁唑啉合成路线 (共 73 条)
反应条件
C2H3O2(1-)*C20H30OP(1-)*C20H31OP*Pd(2+); lithium tert-butylate in N,N-dimethyl acetamide T=100°C; 14 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Barfuesser, Sebastian; Kornhaass, Christoph; Kapdi, Anant R.
Organic Letters, 2011 , vol. 13, # 12 p. 3082 - 3085
参考文献
Journal of the American Chemical Society, , vol. 77, p. 5113,5115
反应条件
[bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane T=0°C; 0.5 h;
参考文献
Kangani, Cyrous O.; Kelley, David E.
Tetrahedron Letters, 2005 , vol. 46, # 51 p. 8917 - 8920
反应条件
1: in chloroform T=80°C; P=206.859 - 517.148 Torr; 0.166667 h; microwave irradiation; 2: With thionyl chloride in chloroform T=80°C; 0.0333333 h; microwave irradiation;
参考文献
Katritzky, Alan R.; Cai, Chunming; Suzuki, Kazuyuki; Singh, Sandeep K.
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 811 - 814
反应条件
copper(II) bis(trifluoromethanesulfonate); diisopropyl-carbodiimide in 1,4-dioxane 5 h; Heating;
参考文献
Crosignani, Stefano; Young, Abigail C.; Linclau, Bruno
Tetrahedron Letters, 2004 , vol. 45, # 52 p. 9611 - 9615
反应条件
1: in dichloromethane T=20°C; 18 h; 2: With thionyl chloride in dichloromethane Further stages.;
参考文献
Clayden, Jonathan; Stimson, Christopher C.; Keenan, Martine
Chemical Communications, 2006 , # 13 p. 1393 - 1394
反应条件
[RhCl(cis-cyclooctene)2]2; triethylamine; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=105°C; 18 h;
参考文献
Lewis, Jared C.; Wiedemann, Sean H.; Bergman, Robert G.; Ellman, Jonathan A.
Organic Letters, 2004 , vol. 6, # 1 p. 35 - 38
反应条件
1: With Ph2CuLi*LiCN in diethyl ether T=0°C; 0.5 h; 2: With water; ammonium chloride in diethyl ether
参考文献
Cetin, Fatma; Baris Senogul; Gezer, Sibel; Astley, Demet; Astley, Stephen T.
Journal of Organometallic Chemistry, 2004 , vol. 689, # 1 p. 154 - 157
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether 16 h; Ambient temperature;
参考文献
Pridgen, Lendon N.; Killmer, Lewis B.
Journal of Organic Chemistry, 1981 , vol. 46, # 26 p. 5402 - 5404
反应条件
1: in diethyl ether T=0°C; 0.5 h; 2: With water; ammonium chloride in diethyl ether
参考文献
Journal of Organometallic Chemistry, , vol. 689, # 1 p. 154 - 157