2-溴乙基4-甲基苯磺酸盐合成路线 （共 14 条）
反应条件
pyridine T=20°C; 2 h;
参考文献
Nanno, Tetsuo; Deguchi, Masaki
Patent: US2008/306308 A1, 2008 ;
Location in patent: Page/Page column 8 ;
参考文献
Iwata, Masaaki; Kuzuhara, Hiroyoshi
Journal of the Chemical Society, Chemical Communications, 1985 , # 13 p. 918 - 919
反应条件
bromine; TBA p-toluenesulfonate in dichloromethane T=20°C;
参考文献
Zefirov, N. S.; Koz'min, A. S.; Dan'kov, Yu. V.; Zhdankin, V. V.; Kirin, V. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 205 - 213
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 233 - 242
反应条件
triethylamine in dichloromethane ice-cooling;
参考文献
Tada, Masaru; Shijima, Hiroyasu; Nakamura, Masaharu
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 14 p. 2499 - 2505
反应条件
tetrabutylammomium bromide T=120 - 135°C; 2 h; other alkyl halides and alkyl sulfonates; Product distribution;
参考文献
Hahn, Roger C.; Tompkins, Jan
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5783 - 5785
反应条件
bromine in dichloromethane T=20°C; Product distributionMechanism;
参考文献
Zefirov, N.S.; Koz'min, A.S.; Dan'kov, Yu.V.; Zhdankin, V.V.; Kirin, V.N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1750 - 1751
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 9 p. 1993 - 1994
参考文献
Titow; Makljaew
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 1631,1634;engl.Ausg.S.1613
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 12 h; Heating;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 14 p. 2499 - 2505
反应条件
in N,N-dimethyl-formamide T=50°C;
参考文献
Chemistry Letters, , p. 369 - 372
反应条件
potassium carbonate in N,N-dimethyl-formamide 68 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 6 p. 2394 - 2411
