二(4-甲氧基苯基)-溴化碘(1:1)合成路线 (共 11 条)
反应条件
iodosyl sulfate; acetic acid anschliessend Behandeln mit wss. Natriumbromid-Loesung;
参考文献
Azoo,J.A. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2521 - 2522
反应条件
1: para-iodoanisole With sodium perborate; acetic anhydride T=40°C; 1.5 h; 2: methoxybenzene With sulfuric acid T=15°C; 5 h; 3: With potassium bromide
参考文献
Kryska, Anna; Skulski, Lech
Molecules, 2001 , vol. 6, # 11 p. 875 - 880
反应条件
1: Et3N, Cu / methanol 2: HI, AcOH 3: I2, KI, aq. EtNH2 View Scheme
参考文献
Blank; Rice; Pfeiffer; Greenberg
Journal of medicinal chemistry, 1966 , vol. 9, # 1 p. 10 - 15
反应条件
T=60°C; sowie 80grad und 100grad; Zersetzung; Rate constant;
参考文献
Beringer; Mausner
Journal of the American Chemical Society, 1958 , vol. 80, p. 4535
反应条件
sodium hydride; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=40°C;
参考文献
Wang, Feng-Yan; Chen, Zhen-Chu; Zheng, Qin-Guo
Journal of Chemical Research, 2004 , # 3 p. 206 - 207
反应条件
1: Et3N, Cu 2: aq. HI, AcOH View Scheme
参考文献
Jorgensen,E.C. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 3396 - 3398
反应条件
methanol; magnesium methanolate
参考文献
Hillmann
Patent: US2886592 , 1957 ;
反应条件
T=60°C; sowie 80grad und 100grad; Zersetzung; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 4535
反应条件
zinc; bis(acetylacetonato) palladium in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1165 - 1166
反应条件
sodium hydride; 1-n-butyl-3-methylimidazolium tetrafluoroborate
T=40°C;
参考文献
Wang, Feng-Yan; Chen, Zhen-Chu; Zheng, Qin-Guo
Journal of Chemical Research, 2004 , # 3 p. 206 - 207