反应条件
diethyl ether in dichloromethane with exclusion of light, molar ratio of starting materials is 1:1, room temp., 5 min; evapn. to dryness, addn. of Et2O, filtration, evapn. to dryness, treated with hexane, drying in vac., elem. anal.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , # 9 p. 2253 - 2264
