5-甲基苯并呋喃-1-氧化物合成路线 （共 23 条）
反应条件
sodium hypochlorite; sodium hydroxide in ethanol; water T=4°C; 0.666667 h;
参考文献
de Carvalho, Paulo Sergio; Marostica, Marta; Gambero, Alessandra; Pedrazzoli Jr., Jose
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 6 p. 2489 - 2493
参考文献
Dyall, Leonard K.
Australian Journal of Chemistry, 1986 , vol. 39, # 1 p. 89 - 101
参考文献
Journal of Medicinal Chemistry, , vol. 11, # 2 p. 305 - 311
反应条件
1: conc. sulfuric acid / 0.25 h / 100 °C 2: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min 3: toluene / 2 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 10 p. 1786 - 1792
反应条件
1: acetic acid / 0.25 h / Heating 2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min 3: conc. sulfuric acid / 0.25 h / 100 °C 4: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min 5: toluene / 2 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 10 p. 1786 - 1792
反应条件
1: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min 2: conc. sulfuric acid / 0.25 h / 100 °C 3: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min 4: toluene / 2 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 10 p. 1786 - 1792
反应条件
1: 1.) aq. HCl, NaNO2, 2.) NaN3, aq. AcONa / 1.) from 2 to 4 deg C, 15 min, 2.) 0 deg C, 30 min 2: 94.5 percent Spectr. / decahydronaphthalene / 87.7 °C / ΔE(excit.), ΔS(excit.) View Scheme
参考文献
Australian Journal of Chemistry, , vol. 39, # 1 p. 89 - 101
反应条件
acetic acid; benzene
参考文献
Australian Journal of Chemistry, , vol. 11, p. 485,487
反应条件
1: hydrochloric acid; NaNO2 View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 307, p. 43
反应条件
acetic acid; benzene
参考文献
Journal of the Chemical Society, , p. 4499,4501
Australian Journal of Chemistry, , vol. 11, p. 485,486
