2-苯基-2H-苯并噻唑合成路线 （共 42 条）
反应条件
potassium carbonate; L-proline; copper(l) chloride in dimethyl sulfoxide
T=160°C; 0.5 h; Microwave irradiation; regioselective reaction;
参考文献
Liu, Yuxiu; Yan, Wuming; Chen, Yunfeng; Petersen, Jeffrey L.; Shi, Xiaodong
Organic Letters, 2008 , vol. 10, # 23 p. 5389 - 5392
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide; potassium carbonate; [Pd(1,2-bis(diphenylphosphino)ethane)Cl2] in N,N-dimethyl-formamide
T=150°C; 8 h;
参考文献
Beletskaya, Irina P.; Davydov, Dmitri V.; Moreno-Manas, Marcial
Tetrahedron Letters, 1998 , vol. 39, # 31 p. 5617 - 5620
反应条件
3,4,5,6-tetramethyl-t-Bu-X-Phos; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
T=120°C; 5 h; Inert atmosphere;
参考文献
Ueda, Satoshi; Su, Mingjuan; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 38 p. 8944 - 8947
反应条件
potassium hydroxide; potassium tert-butylate in pyridine
T=20°C; 17 h;
参考文献
Brown, Richard A.; Fernando, Sharon I. S.; Roberts, Roger M. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 2 p. 197 - 202
反应条件
in various solvent(s)
0.0166667 h; Heating;
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
in various solvent(s)
9 h; Heating;
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
sodium dithionite; ethanol; sodium hydrogensulfite
参考文献
Grandmougin
Journal fuer Praktische Chemie (Leipzig), 1907 , vol. <2> 76, p. 140
Chem. Zentralbl., 1908 , vol. 79, # I p. 2178
反应条件
1: phosphorus pentachloride / toluene / Ambient temperature
2: 81 percent / hydroxylamine / 1,2-dimethoxy-ethane; diethyl ether / 26 h / Ambient temperature
3: 67 percent / thionyl chloride / benzene / 1 h / Ambient temperature
4: 90 percent / various solvent(s) / 1 h / Heating
View Scheme
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
1: 81 percent / hydroxylamine / 1,2-dimethoxy-ethane; diethyl ether / 26 h / Ambient temperature
2: 67 percent / thionyl chloride / benzene / 1 h / Ambient temperature
3: 90 percent / various solvent(s) / 1 h / Heating
View Scheme
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
1: 67 percent / thionyl chloride / benzene / 1 h / Ambient temperature
2: 90 percent / various solvent(s) / 1 h / Heating
View Scheme
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
