1-(2-丙炔基)环己烷-1-醇合成路线 （共 25 条）
反应条件
sodium hydroxide in water
0.5 h; Heating;
参考文献
Leyssens; Van Boven; Daenens
Pharmazie, 1984 , vol. 39, # 2 p. 114 - 117
反应条件
potassium fluoride; titanium tetrachloride
1) CH2Cl2 a) -78 deg C b) -> 25 deg C, 2h 2) DMSO, 25 deg C, 4h; Yield given. Multistep reaction;
参考文献
Danheiser, Rick L.; Carini, David J.
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3925 - 3927
反应条件
methyllithium
1) THF, -95 deg C, 10 min 2) -95 deg C, 20 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Suzuki, Masaaki; Morita, Yasushi; Noyori, Ryoji
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 441 - 449
反应条件
sodium hydroxide; dihydrogen peroxide
1) Et2O, 25 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Khire, Uday R.; Racherla, Uday S.
Tetrahedron Letters, 1993 , vol. 34, # 1 p. 15 - 18
反应条件
in methanol
48 h; Heating; Title compound not separated from byproducts.;
参考文献
McCluskey; Muderawan; Muntari; Young
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7811 - 7817
反应条件
tetrahydrofuran; aluminium amalgam
anschliessendes Erwaermen mit Cyclohexanon und Aether;
参考文献
Laeuger et al.
Helvetica Chimica Acta, 1959 , vol. 42, p. 2379,2388
反应条件
diethylzinc
1.) ether, 0 deg C, 2.) ether, 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shinokubo, Hiroshi; Miki, Hiroaki; Yokoo, Toshiaki; Oshima, Koichiro; Utimoto, Kiitiro
Tetrahedron, 1995 , vol. 51, # 43 p. 11681 - 11692
反应条件
Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Khire, Uday R.; Narla, Gowriswari; Racherla, Uday S.
Journal of Organic Chemistry, 1995 , vol. 60, # 3 p. 544 - 549
参考文献
Henbest; Jones; Walls
Journal of the Chemical Society, 1949 , p. 2696,2698
反应条件
sodium hydroxide; 1,4-bismaleimidobutane; dihydrogen peroxide
Yield given. Multistep reaction;
参考文献
Dana, Gilbert; Figadere, Bruno; Touboul, Estera
Tetrahedron Letters, 1985 , vol. 26, # 46 p. 5683 - 5684
