2-甲基-3-二甲氨基-2-丙烯醛合成路线 （共 10 条）
反应条件
trichlorophosphate 1.) <30 deg C, 2.) 70 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 3030
反应条件
potassium carbonate; trichlorophosphate 1.) 1,2-dichloroethane, room temperature, 15 min, then 0 deg C and 70 deg C, 40 min, 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 43, # 1 p. 171 - 178
反应条件
1,2-dichloro-ethane und Behandeln des Reaktionsgemisches mit Propionaldehyd-diaethylacetal;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 23, p. 452,455
反应条件
oxalyl dichloride; potassium carbonate multistep reaction; reaction with other 1,1-diethoxyalkanes;
参考文献
Tetrahedron, , vol. 43, # 1 p. 171 - 178
反应条件
1: With potassium tert-butylate in tetrahydrofuran T=40°C; Michael reaction; 0.166667 h; 2: With ammonium acetate; acetic acid T=90°C; 3 h;
参考文献
Kuwabara, Hirokazu; Umihara, Ken; Furugori, Yasushi; Itoh, Isamu
Chemistry Letters, 2005 , vol. 34, # 6 p. 834 - 835
反应条件
2: Me2NH / 1 h / 75 - 78 °C View Scheme
参考文献
Krasnaya, Zh. A.; Stytsenko, T. S.; Bogdanov, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 96 - 100
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 106 - 111
反应条件
4-toluenesulfonyl azide 1.) 0 deg C, 0.01 Torr, 3 h, 2.) room temperature, 4 h, 3.) 40 deg C, 2 h, atmospheric pressure; Yield given;
参考文献
Menicagli, Rita; Malanga, Corrado; Guidi, Maurizio; Lardicci, Luciano
Tetrahedron, 1987 , vol. 43, # 1 p. 171 - 178
参考文献
Arnold,Z.; Zemlicka,J.
Collection of Czechoslovak Chemical Communications, 1960 , vol. 25, p. 1318 - 1323
反应条件
chloroform Behandeln des Reaktionsprodukts mit Wasser;
参考文献
Arnold; Zemlicka
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 2385,2390
反应条件
sodium hydroxide Behaldeln des erhaltenen Natrium-Salzes mit Chlorwasserstoff in Aether;
参考文献
Arnold; Sorm
Collection of Czechoslovak Chemical Communications, 1958 , vol. 23, p. 452,455
