1: 1-Bromo-2-isopropyl-benzene With magnesium in tetrahydrofuran 5 h; RefluxInert atmosphere; 2: iodine in tetrahydrofuran T=20°C; Inert atmosphere;

copper(l) iodide; sodium iodide; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=110°C; 20 h;

sulfuric acid; iodine cloride T=95 - 100°C; Iodination; 3 h; Title compound not separated from byproducts;

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in N,N-dimethyl-formamide T=60°C; Sealed tube;

1: bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Negishi coupling reaction; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=-78 - 20°C; Negishi coupling reaction; Inert atmosphere; 3: 2-isopropylphenyl iodide With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; hexane T=60°C; Negishi coupling reaction; 2 h; Inert atmosphere;

copper(I) oxide; 4,7-Dimethoxy-1,10-phenanthroline; caesium carbonate; ethylene glycol; poly(ethylene glycol) in various solvent(s) T=110°C; 48 h;

1: 2-isopropylphenyl iodide With magnesium in diethyl ether T=20°C; 2: ethyl isoformanilide in diethyl ether T=20°C;

sulfuric acid; nitric acid in chloroform; water T=20°C; 16 h;

palladium diacetate; CsO2CCMe3 in N,N-dimethyl-formamide T=105°C; 8 h; Inert atmosphere;