(2,3-二叠氮基丙基)-氨基甲酸1,1-二甲基乙基酯合成路线 （共 3 条）
反应条件
sodium azide in N,N-dimethyl-formamide T=80°C; 3 h;
参考文献
Sabbatini, Fabio M.; Fabio, Romano Di; Griffante, Cristiana; Pentassuglia, Giorgio; Zonzini, Laura; Melotto, Sergio; Alvaro, Giuseppe; Capelli, Anna M.; Pippo, Lara; Perdona', Elisabetta; Denis, Yves St.; Costa, Silvano; Corsi, Mauro
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 2 p. 623 - 627
反应条件
1: 87 percent / ethanol / 1 h / Ambient temperature 2: 69 percent / Et3N / CH2Cl2 / 1.) 0 deg C, 1 h, 2.) r.t., 30 min 3: 69 percent / NaN3, 15-crown-5 / dimethylformamide / 12 h / 60 - 70 °C View Scheme
参考文献
Benoist, Eric; Loussouarn, Anthony; Remaud, Patricia; Chatal, Jean-Francois; Gestin, Jean-Francois
Synthesis, 1998 , # 8 p. 1113 - 1118
反应条件
1: 69 percent / Et3N / CH2Cl2 / 1.) 0 deg C, 1 h, 2.) r.t., 30 min 2: 69 percent / NaN3, 15-crown-5 / dimethylformamide / 12 h / 60 - 70 °C View Scheme
参考文献
Benoist, Eric; Loussouarn, Anthony; Remaud, Patricia; Chatal, Jean-Francois; Gestin, Jean-Francois
Synthesis, 1998 , # 8 p. 1113 - 1118
