alpha,alpha-二甲基环己烷甲胺合成路线 （共 3 条）
反应条件
cerium(III) chloride in tetrahydrofuran; diethyl ether T=-10 - 0°C; 1 h;
参考文献
Limanto, John; Dorner, Benjamin; Devine, Paul N.
Synthesis, 2006 , # 24 p. 4143 - 4150
反应条件
1: in tetrahydrofuran; diethyl ether T=100°C; Double Grignard addition; 0.166667 h; Microwave irradiation; 2: With titanium(IV) isopropylate in tetrahydrofuran; diethyl ether T=50°C; Double Grignard addition; 1 h; Microwave irradiation;
参考文献
Wang, Ruifang; Gregg, Brian T.; Zhang, Wei; Golden, Kathryn C.; Quinn, John F.; Cui, Peng; Tymoshenko, Dmytro O.
Tetrahedron Letters, 2009 , vol. 50, # 50 p. 7070 - 7073
反应条件
(i) NaCN, H2SO4, AcOH, (ii) aq. HCl; Multistep reaction;
参考文献
Drefahl,G. et al.
Journal fuer Praktische Chemie (Leipzig), 1964 , vol. 23, p. 136 - 142
