反应条件
in tetrahydrofuran; diethyl ether
Li salt in ether was rapidly added to soln. of W complex in THF at -30°C (N2), react. time 3 h; filtration through Celite, evapn., extn. with pentane, filtration, evapn., sublimation in vac., pptn. with MeCN from Et2O soln.; elem. anal.;
参考文献
Schrock, R. R.; Clark, D. N.; Sancho, J.; Wengrovius, J. H.; Rocklage, S. M.; Pedersen, S. F.
Organometallics, 1982 , vol. 1, p. 1645 - 1651
