2-(4-戊烯)丙二酸二乙酯合成路线 （共 29 条）
反应条件
sodium in ethanol 3 h; Heating;
参考文献
Salomon; Coughlin; Ghosh; Zagorski
Journal of the American Chemical Society, 1982 , vol. 104, # 4 p. 998 - 1007
反应条件
ethylaluminum dichloride in dichloromethane T=0°C;
参考文献
Bambal, Ramesh; Kemmitt, Raymond D. W.
Journal of the Chemical Society, Chemical Communications, 1988 , # 11 p. 734 - 735
反应条件
sodium; acetic acid in ethanol
参考文献
Beecham Group Limited
Patent: US4367338 A1, 1983 ;
反应条件
1: diethyl malonate With sodium hydride in tetrahydrofuran T=0 - 20°C; 1 h; Inert atmosphere; 2: 5-bromo-1-pentene T=20°C; 12 h; Inert atmosphere;
参考文献
Kotha, Sambasivarao; Shirbhate, Mukesh E.
Synlett, 2012 , vol. 23, # 15 p. 2183 - 2188
反应条件
1: pyridine; phosphorus tribromoide / -30 - -25 °C / weniger gut bei Kuehlung mit Eis 2: ethanol View Scheme
参考文献
Julia,M.; Maumy,M.
Bulletin de la Societe Chimique de France, 1969 , p. 2415 - 2427
反应条件
sodium ethanolate in ethanol
参考文献
Brace,N.O.
Journal of Organic Chemistry, 1967 , vol. 32, p. 430 - 434
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=25°C; Cooling with liquid nitrogenSealed tubeUV-irradiation; Kinetics; TemperatureConcentration;
参考文献
Beckwith, Athelstan L. J.; Schiesser, Carl H.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 6 p. 1736 - 1743
反应条件
1: sodium-potassium; diethyl ether / und Zersetzen mit kaltem Wasser oder Eis 2: pyridine; phosphorus tribromoide / -30 - -25 °C / weniger gut bei Kuehlung mit Eis 3: ethanol View Scheme
参考文献
Gaubert; Linstead; Rydon
Journal of the Chemical Society, 1937 , p. 1973
反应条件
1: sodium-potassium; diethyl ether / und Zersetzen mit kaltem Wasser oder Eis 2: pyridine; phosphorus tribromoide / -30 - -25 °C / weniger gut bei Kuehlung mit Eis 3: ethanol View Scheme
参考文献
Gaubert; Linstead; Rydon
Journal of the Chemical Society, 1937 , p. 1973
参考文献
Gaubert; Linstead; Rydon
Journal of the Chemical Society, 1937 , p. 1973
