3-二甲氨基-2,2-二甲基-1-丙醇合成路线 (共 9 条)
反应条件
methanol; platinum Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 61, p. 1200,1201
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2593
参考文献
Bulletin de la Societe Chimique de France, , vol. <4>47, p. 869
反应条件
1: 1.) n-BuLi, 2,2,6,6-tetramethylpiperidine / 1.) THF, HMPA, hexane, 0 deg C, 20 min, 2.) THF, HMPA, hexane, 10 deg C, 15 min and 45 deg C, 30 min 2: 47 percent / BF3*Et2O, borane-dimethyl sulfide / tetrahydrofuran / 0.5 h / 0 - 45 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 12 p. 2787 - 2793
反应条件
methanol; sodium iodide T=170°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 16, p. 751,759
Chem.Abstr., , p. 2033
参考文献
Journal of Organic Chemistry, , vol. 26, p. 686 - 691
反应条件
sodium in benzene
Heating;
参考文献
Newman; Broger; LaPidus; Tye
Journal of medicinal chemistry, 1972 , vol. 15, # 10 p. 1003 - 1006
参考文献
Mannich
Patent: DE571295 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 3024
Full Text Show Details
Lesser,B.
Diss. <Frankfurt a. M. 1930> S. 18
反应条件
(i) NaH, benzene, (ii) /BRN= 1912198/; Multistep reaction;
参考文献
Newman; Broger; LaPidus; Tye
Journal of medicinal chemistry, 1972 , vol. 15, # 10 p. 1003 - 1006