2-(1,3-苯并噻唑-2-基)硫代乙酰胺合成路线 (共 7 条)
反应条件
hydrogen sulfide; sodium methylate in isopropyl alcohol T=60°C; 3 h;
参考文献
Domasevich
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 4 p. 569 - 570
反应条件
hydrogenchloride in N,N-dimethyl-formamide T=90 - 100°C; 2 h;
参考文献
Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 11 p. 2856 - 2869
反应条件
Lawesson's reagent in toluene 2 h; Heating;
参考文献
Abbotto, Alessandro; Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5753 - 5772
反应条件
1: 8.01 g / 30percent aqueous NH3 / ethanol / 18 h / 20 °C 2: Lawesson's reagent / toluene / 2 h / Heating View Scheme
参考文献
Abbotto, Alessandro; Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5753 - 5772
反应条件
1: 2 h / 120 °C 2: 8.01 g / 30percent aqueous NH3 / ethanol / 18 h / 20 °C 3: Lawesson's reagent / toluene / 2 h / Heating View Scheme
参考文献
Abbotto, Alessandro; Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5753 - 5772
反应条件
acetic acid 1.5 h; Heating;
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2834 - 2849
反应条件
1: 78 percent / methanol / 3 h / Heating 2: AcOH / 1 h / Heating View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2834 - 2849