1-(1-甲基-1H-吲哚-3-基)-1-乙酮合成路线 (共 29 条)
反应条件
1: propionic acid anhydride / 100 °C 2: sodium hydroxide / water / 3.5 h / Reflux 3: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 0.33 h / 20 °C View Scheme
参考文献
Letters in Organic Chemistry, , vol. 8, # 9 p. 656 - 662
反应条件
diethylaluminium chloride in hexane; dichloromethane T=0°C; 0.5 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 4 p. 1047 - 1060
反应条件
1: sodium hydroxide / water / 3.5 h / Reflux 2: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 0.33 h / 20 °C View Scheme
参考文献
Letters in Organic Chemistry, , vol. 8, # 9 p. 656 - 662
反应条件
1: 98 percent / KOH / methanol / 0.05 h / Heating 2: 25 percent / acetonitrile / 1 h / Heating 3: 38 percent / KOH / methanol; H2O View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 18, # 2 p. 164 - 169
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 18, # 2 p. 212 - 218
反应条件
1: 25 percent / acetonitrile / 1 h / Heating 2: 38 percent / KOH / methanol; H2O View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 18, # 2 p. 164 - 169
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 18, # 2 p. 212 - 218
反应条件
in N,N-dimethyl-formamide T=110°C; 4 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 4 p. 793 - 801
反应条件
potassium carbonate in water 4 h; RefluxInert atmosphere;
参考文献
Synthesis, , # 5 art. no. M05709SS, p. 775 - 782
反应条件
potassium carbonate in toluene 24 h; Inert atmosphereReflux;
参考文献
Synthesis, , # 5 art. no. M05709SS, p. 775 - 782
反应条件
sodium hydroxide; ethanol; water
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 22, p. 1063
反应条件
sodium hydroxide; water
参考文献
Sb. Statei Obshch. Khim., , p. 712
Chem.Abstr., , p. 1006